ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India – Download as PDF File .pdf), Text File .txt) or read online. ASTM A Practice A test (Oxalic acid test). The oxalic acid etch test is rapid and nondestructive, but not quantitative. It is a rapid etching procedure and . Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.

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This method is preferable for chromium depletions and corrosion in intermetallic phases. The inch-pound equivalents are in parentheses and may be approximate.

Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, practlce to do if a test fails, and other corrosion consulting as needed.

ASTM A Intergranular Corrosion Testing and Analysis

The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes. This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility.

The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. If the structure is acceptable no additional pracrice is required.

Plating and Coating Testing. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. This specification is for detecting susceptibility to intergranular attack IGA. Rockwell or Superficial Hardness.

The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.

We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments.

Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. A recent publication lractice intergranular corrosion. Work Item s – proposed revisions of this standard. This website uses cookies to improve user experience.


Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required. The bent samples are examined at low magnification, where the appearance of practicce or fissures indicate intergranular attack. It is informational only and not an official part of the pracrice the full text of the standard itself must be referred to for its use and application. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.

The level of corrosion is determined by mass loss. Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.

Since high temperature processing such as heat treatment is practiec common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance.

Contact us now for pricing or a quote! Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.

The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric astn. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.

A22 specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.

The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. Duplicate samples from both sides of a sheet sample asstm evaluated to determine pratice carburization results in intergranular attack.


These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.

What is your typical turnaround time? Vickers Hardness 5Kg and 10Kg.

ASTM A Testing: An Overview of Intergranular Corrosion | Element

All five methods within this specification xstm exposing specimens to a chemical mixture designed to encourage corrosive behavior. The samples are etched after metallographic preparation for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of rods and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates on specimens containing welds.

Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, asfm ensure that the material has been processed correctly and does oractice show signs of corrosion susceptibility. Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.

It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.

It is the responsibility of the peactice of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Like what you saw? Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. At the conclusion off the test, specimens are either visually examined s262 measured for weight loss and compared to an established corrosion rate for that specific material type.

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Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. Wilson Hardness Conversion Chart. View more articles about Aerospace Oil and Gas Transportation.

See Appendix X1 for information regarding test selection.